EXTRACTABLE COPPER AND ZINC WITH MEHLICH-1 AND MEHLICH-3 IN SOILS FERTILIZED WITH SWINE MANURE

Authors

  • João Carlos Arruda-Oliveira oliveira.joao@ifmt.edu.br
    Instituto Federal de Educação, Ciência e Tecnologia de Mato Grosso, Juína, MT, Brasil. / Programa de Pós-Graduação em Agricultura Tropical, Universidade Federal de Mato Grosso, Cuiabá, MT, Brasil. https://orcid.org/0000-0001-5833-2823
  • Josimar Brito Silva britoptga@gmail.com
    Secretaria de Estado de Meio Ambiente de Mato Grosso, Cuiabá, MT, Brasil. / Programa de Pós-Graduação em Agricultura Tropical, Universidade Federal de Mato Grosso, Cuiabá, MT, Brasil. https://orcid.org/0000-0002-3137-8853
  • Emerson Silva Miranda s.emersonmiranda@gmail.com
    Programa de Pós-Graduação em Ciência Animal, Universidade Federal de Mato Grosso, Cuiabá, MT, Brasil. https://orcid.org/0009-0009-0029-3505
  • Henrique Ferreira Araujo henrique.santana.ferreira@gmail.com
    Programa de Pós-Graduação em Agricultura Tropical, Universidade Federal de Mato Grosso, Cuiabá, MT, Brasil. https://orcid.org/0009-0005-5892-397X
  • Renata Vilalba Reis renata-vilalba@hotmail.com
    Programa de Pós-Graduação em Agricultura Tropical, Universidade Federal de Mato Grosso, Cuiabá, MT, Brasil. https://orcid.org/0000-0002-8040-7841
  • Jholian Maicon Ribeiro-Santos jholianmaicon@gmail.com
    Programa de Pós-Graduação em Agricultura Tropical, Universidade Federal de Mato Grosso, Cuiabá, MT, Brasil. https://orcid.org/0000-0003-2081-0353
  • Josias do Espírito Santo Coringa josias.coringa@ifmt.edu.br
    Instituto Federal de Educação, Ciência e Tecnologia de Mato Grosso, Cuiabá, MT, Brasil. https://orcid.org/0000-0001-9489-8234
  • Oscarlina Lúcia Santos Weber oscarlinaweber@gmail.com
    Programa de Pós-Graduação em Agricultura Tropical, Universidade Federal de Mato Grosso, Cuiabá, MT, Brasil. https://orcid.org/0000-0002-0625-4904

DOI:

https://doi.org/10.31413/nat.v14i4.21569


Keywords:

efluentes suínos, micronutrientes, métodos de extração, solos arenosos

Abstract

This study aimed to evaluate the ability of the Mehlich-1 (M1) and Mehlich-3 (M3) extractants to determine extractable Cu and Zn contents in agricultural soils of the Mato Grosso Cerrado with a management history of liquid swine manure (DLS). The sampled areas, with sandy loam and sandy textures, were divided into four 15 ha plots each, with soil sampling conducted at three depths (0.00–0.05; 0.05–0.10; and 0.10–0.20 m). The collected data did not meet normality assumptions and were analyzed using non-parametric methods (Mann-Whitney and Kruskal-Wallis), adopting a 5% significance level. For Cu, both extractants showed similar performance in sandy loam soils, while M3 demonstrated greater efficiency in sandy soils. In contrast, M1 exhibited higher extraction capacity for Zn in both textural classes. Despite differences in extraction magnitude, a significant correlation was observed between the concentrations determined by M1 and M3 for both nutrients. The results suggest that in Cerrado soils managed with DLS, extractant efficiency depends both on soil texture class and on the specific chemical affinity of each element.

References

ALVARES, C. A.; STAPE, J. L.; SENTELHAS, P. C.; GONÇALVES, J. L. de M.; SPAROVEK, G. Köppen's climate classification map for Brazil. Meteorologische Zeitschrift, v. 22, n. 6, p. 711-728, 2013. https://doi.org/10.1127/0941-2948/2013/0507

ANTONANGELO, J. A.; SOUZA, J. L. B.; WHITAKER, A.; ARNALL, B.; ZHANG, H. Evaluation of Mehlich-3 as a multi-element extractor for micronutrients and sulfur in a soil–ryegrass system amended with variable biochar rates from two feedstocks. Land, v. 11, n. 11, e1979, 2022. https://doi.org/10.3390/land11111979

ARRUDA-OLIVEIRA, J. C.; SILVA, J. B.; MIRANDA, E. S.; RIBEIRO-SANTOS, J. M.; WEBER, O. L. S. Performance of Mehlich-1 and Mehlich-3 extractors in quantifying phosphorus in soils fertilized with liquid swine manure. Bioagro, v. 36, n. 2, p. 237-244, 2024. https://doi.org/10.51372/bioagro362.11

BROOM, L. J.; MONTEIRO, A.; PIÑÓN, A. Recent advances in understanding the influence of zinc, copper, and manganese on the gastrointestinal environment of pigs and poultry. Animals, v. 11, n. 5, e1276, 2021. https://doi.org/10.3390/ani11051276

CARVALHO, M. L.; MACIEL, V. F.; BORDONAL, R. de O.; CARVALHO, J. L. N.; FERREIRA, T. O.; CERRI, C. E. P.; CHERUBIN, M. R. Stabilization of organic matter in soils: drivers, mechanisms, and analytical tools - a literature review. Revista Brasileira de Ciência do Solo, v. 47, e20220130, 2023. https://doi.org/10.36783/18069657rbcs20220130

DALTO, D. B.; LAPOINTE, J.; MATTE, J. J. Swine nutrition and trace mineral supplementation: environmental impacts and physiological considerations. Journal of Animal Science, v. 101, e312, 2023. https://doi.org/10.1093/jas/skad312

FLORENTINO, R. W.; KUMMER, A. C. B.; BEDNARZ, J. A.; MARTINS, K. G. Influence of liquid swine slurry on soil quality and water infiltration. Revista Brasileira de Ciências Ambientais, v. 60, e2301, 2025. https://doi.org/10.5327/Z2176-94782301

GÜRBÜZ, M. A. Identification of multiple extraction methods to be used in extraction of macro and micronutrients of neutral and alkaline soils by a multi-criteria decision-making technique (TOPSIS). Journal of Soil Science and Plant Nutrition, v. 25, p. 4669–4686, 2025. https://doi.org/10.1007/s42729-025-02422-y

LOURENZI, C. R.; SCHERER, E. E.; CERETTA, C. A.; TIECHER, T. L.; CANCIAN, A.; FERREIRA, P. A. A.; BRUNETTO, G. Atributos químicos de Latossolo após sucessivas aplicações de composto orgânico de dejeto líquido de suínos. Pesquisa Agropecuária Brasileira, v. 51, n. 3, p. 233-242, 2016. https://doi.org/10.1590/S0100-204X2016000300005

MARTÍNEZ, E.; MARESMA, A.; BIAU, A.; BERENGUER, P.; CELA, S.; SANTIVERI, F.; MICHELENA, A.; LLOVERAS, J. Long-term effects of liquid swine manure on soil organic carbon and Cu/Zn levels in soil and maize. Nutrient Cycling in Agroecosystems, v. 118, p. 193-205, 2020. https://doi.org/10.1007/s10705-020-10093-7

MEHLICH, A. Mehlich 3 soil test extractant: a modification of Mehlich 2 extractant. Communications in Soil Science and Plant Analysis, v. 15, n. 12, p. 1409-1416, 1984. https://doi.org/10.1080/00103628409367568

MEHLICH, A. New extractant for soil test evaluation of phosphorus, potassium, magnesium, calcium, sodium, manganese and zinc. Communications in Soil Science and Plant Analysis, v. 9, n. 6, p. 477-492, 1978. https://doi.org/10.1080/00103627809366824

MENEZES, A. A.; DIAS, L. E.; NEVES, J. C. L.; SILVA, J. V. O. da. Disponibilidade de zinco para milho pelos extratores Mehlich-1, Mehlich-3 e DTPA em solos de Minas Gerais, na presença e ausência de calagem. Revista Brasileira de Ciência do Solo, v. 34, n. 2, p. 417-424, 2010. https://doi.org/10.1590/S0100-06832010000200015

R CORE TEAM. R: a language and environment for statistical computing. Vienna: R Foundation for Statistical Computing, 2026. https://www.R-project.org/

SANDHU, A. K.; SHARMA, A.; KAUR, N.; ZOTARELLI, L.; MORGAN, K.; SHARMA, L. K. Evaluate the use of Mehlich-III compared to Mehlich-I as a soil test in Northeast Florida. Farming System, v. 1, n. 3, e100056, 2023. https://doi.org/10.1016/j.farsys.2023.100056

SANTOS, H. G. dos; JACOMINE, P. K. T.; ANJOS, L. H. C. dos; OLIVEIRA, V. A. de; LUMBRERAS, J. F.; COELHO, M. R.; ALMEIDA, J. A. de; ARAUJO FILHO, J. C. de; OLIVEIRA, J. B. de; CUNHA, T. J. F. Sistema Brasileiro de Classificação de Solos. 5 ed. Brasília: Embrapa, 2018. 356p.

SCHONINGER, E. L.; GATIBONI, L. C.; LINHARES, D. Método Mehlich 3 como substituinte ao HCl para extração de cobre e zinco em solos com alto teor de matéria orgânica do sul do Brasil. Ciência Rural, v. 42, n. 7, p. 1200-1203, 2012. https://doi.org/10.1590/S0103-84782012000700010

SILVA, F. C. da. Manual de análises químicas de solos, plantas e fertilizantes. 2 ed. Brasília: Embrapa Informação Tecnológica, 2009. 627p.

SILVA, M. A. G. da; MUNIZ, A. S.; NODA, A. Y.; MARCHETTI, M. E.; MATA, J. de D. V. da; LOURENTE, E. R. P. Metodologias e eficiência de extratores para zinco, cobre, ferro e manganês. Acta Scientiarum Agronomy, v. 31, n. 3, p. 537-545, 2009. https://doi.org/10.4025/actasciagron.v31i3.736

SILVA, R. T. da; JESUS, W. A. de; SOARES, M. R. dos S.; BARROS, A. I.; WEBER, O. L. dos S. Efeito das doses de dejeto líquido de suínos nos atributos físicos, químicos e eletroquímicos em um Latossolo do Cerrado. Química Nova, v. 48, n. 1, e20250004, 2024. https://doi.org/10.21577/0100-4042.20250004

TEIXEIRA, P. C.; DONAGEMMA, G. K.; FONTANA, A.; TEIXEIRA, W. G. Manual de métodos de análise de solo. 3. ed. Brasília: Embrapa, 2017. 574p.

TIECHER, T. L.; CERETTA, C. A.; COMIN, J. J.; GIROTTO, E.; MIOTTO, A.; MORAES, M. P. de; BENEDET, L.; FERREIRA, P. A. A.; LORENZI, C. R.; COUTO, R. R.; BRUNETTO, G. Forms and accumulation of copper and zinc in a sandy typic hapludalf soil after long-term application of pig slurry and deep litter. Revista Brasileira de Ciência do Solo, v. 37, n. 3, p. 812-824, 2013. https://doi.org/10.1590/S0100-06832013000300028

ZHANG, R.; LIAO, Z.; LIAN, W.; YUAN, H.; CHEN, Y.; WENG, L. Livestock manure fertilization as a 'source' or a 'sink' of soluble heavy metals in soil: Insights from geochemical modeling. Journal of Hazardous Materials, v. 501, e140912, 2026. https://doi.org/10.1016/j.jhazmat.2025.140912

Published

2026-10-27

Issue

Section

Agronomia / Agronomy

How to Cite

EXTRACTABLE COPPER AND ZINC WITH MEHLICH-1 AND MEHLICH-3 IN SOILS FERTILIZED WITH SWINE MANURE. (2026). Nativa, 14(4), e21569. https://doi.org/10.31413/nat.v14i4.21569

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